Molecularly imprinted polymer applied to the determination of the residual mass of atrazine and metabolites within an agricultural catchment (Brévilles, France) - Archive ouverte HAL Accéder directement au contenu
Article Dans Une Revue Journal of Chromatography A Année : 2008

Molecularly imprinted polymer applied to the determination of the residual mass of atrazine and metabolites within an agricultural catchment (Brévilles, France)

(1) , (1) , (2) , (1)
1
2

Résumé

Atrazine, desethyl-atrazine and desisopropyl-atrazine have been measured in the soils of Brévilles watershed. Pressurised liquid extraction (PLE) technique was used for extraction followed by purification with terbutylazine molecularly imprinted polymers. This clean-up procedure allowed to remove interfering compounds from the sample extracts. Thus making easier the analyses by reversed phase liquid chromatography coupled with ion trap tandem mass spectrometry. This selective sample treatment for soil extracts allowed limit of quantification (LOQ) of 0.03 ng/g for atrazine and 0.05 ng/g for metabolites. The concentrations in soil samples ranged from 7.1 ng/g to

Dates et versions

hal-00643339 , version 1 (21-11-2011)

Identifiants

Citer

Laurence Amalric, Christophe Mouvet, Valérie Pichon, Sébastien Bristeau. Molecularly imprinted polymer applied to the determination of the residual mass of atrazine and metabolites within an agricultural catchment (Brévilles, France). Journal of Chromatography A, 2008, 1206 (2), pp.95-104. ⟨10.1016/j.chroma.2008.08.034⟩. ⟨hal-00643339⟩
105 Consultations
0 Téléchargements

Altmetric

Partager

Gmail Facebook Twitter LinkedIn More